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- Termite Resistance, Chemical and Mechanical Characterization of Paulownia tomentosa Wood before and after Heat TreatmentPublication . Esteves, Bruno M.; Ferreira, Helena; Viana, Hélder; Ferreira, José; Domingos, Idalina J.; Cruz-Lopes, Luísa; Jones, Dennis; Nunes, LinaThe introduction of new species in forest management must be undertaken with a degree of care, to help prevent the spread of invasive species. However, new species with higher profitability are needed to increase forest products value and the resilience of rural populations. Paulownia tomentosa has an extremely fast growth. The objective and novelty of this work was to study the potential use of young Paulownia trees grown in Portugal by using heat treatment to improve its properties, thereby allowing higher value applications of the wood. The average chemical composition of untreated and heat-treated wood was determined. The extractive content was determined by successive Soxhlet extraction with dichloromethane (DCM), ethanol and water as solvents. The composition of lipophilic extracts was performed by injection in GC-MS with mass detection. Insoluble and soluble lignin, holocellulose and α-cellulose were also determined. Physical (density and water absorption and dimensional stability) and mechanical properties (bending strength and bending stiffness) and termite resistance was also determined. Results showed that extractive content increased in all solvents, lignin and α-cellulose also increased and hemicelluloses decreased. Compounds derived from the thermal degradation of lignin were found in heat-treated wood extractions. Dimensional stability improved but there was a decrease in mechanical properties. Resistance against termites was better for untreated wood than for heat-treated wood, possibly due to the thermal degradation of some toxic extractives.
- Assessment of the Density Loss in Anobiid Infested Pine Using X-ray Micro-Computed TomographyPublication . Parracha, João Luís; Pereira, Manuel; Maurício, António; Faria, Paulina; Lima, Daniel F.; Tenório, Marina; Nunes, LinaThe present study aims at evaluating the impact of anobiid damage on pine timber elements. Anobiid attack produces a diffuse damage of the elements with a set of tunnels in random directions and sizes, thus confusing quantification. Therefore, a method was developed based on X-ray micro-computed tomography (μ-XCT) to obtain, for naturally infested timber samples, an empirical correlation between lost material percentage (consumed by beetles) and timber apparent density (original, before degradation—OTD and residual, after degradation—RTD). The quantified density loss can then be used in further assessment of the structure. The results of the tests performed showed high correlation between original apparent density and lost material percentage (r² = 0.60) and between residual apparent density and lost material percentage (r² = 0.83), which confirms μ-XCT as a valuable tool to the required quantification. The loss of density results can be further applied on the definition of an assessment method for the evaluation of the residual strength of anobiids infested timber, thus contributing to reducing unnecessary replacement. The optimized procedure of the μ-XCT study for infested Maritime pine (Pinus pinaster) is presented and discussed in this article.
- Effects of hygrothermal, UV and SO₂ accelerated ageing on the durability of ETICS in urban environmentsPublication . Parracha, João Luís; Borsoi, Giovanni; Veiga, Rosário; Flores-Colen, Inês; Nunes, Lina; Garcia, Ana R.; Ilharco, Laura M.; Dionísio, Amélia; Faria, PaulinaExternal Thermal Insulation Composite Systems (ETICS) have been extensively used for either new constructions or building facades retrofitting in the last decades. These systems can provide improved thermal performance to the building envelope. However, their long-term durability remains a pervasive concern, with some systems presenting relevant anomalies after few years from their application. The durability assessment of ETICS is defined by the EAD 040083-00-0404 guideline, which stated an accelerated ageing procedure based on the hygrothermal and freeze-thaw behaviour. Nevertheless, further important environmental urban conditions, such as UV radiation and atmospheric pollutants, as well as bio-susceptibility, are not envisaged in the guideline. This paper presents the results of an experimental campaign with the aim of evaluating the durability of the rendering system of several commercially available ETICS exposed to an innovative accelerated ageing procedure, which consists of hygrothermal cycles, UV radiation and air pollutants (SO₂) exposure. Physical and chemical-morphological tests were carried out prior and after each ageing cycle in order to evaluate the durability of ETICS. Biological susceptibility to moulds was also assessed. The experimental results showed that both surface hardness and surface gloss decreased after the combined effect of the hygrothermal, UV, and SO₂ ageing cycles, whereas an increase of surface roughness was observed. Substantial colour change for all systems after the ageing procedure was observed, confirming aesthetic alteration. Traces of biological growth were detected on the systems after ageing and the contact angle decreased after the hygrothermal cycles, indicating a lower surface hydrophobicity of the systems.
- Agro-industrial wastes as building insulation materials : A review and challenges for Euro-Mediterranean countriesPublication . Cintura, Eleonora; Nunes, Lina; Esteves, Bruno M.; Faria, PaulinaThis study investigates the possibility of using agro-industrial wastes for building products, mainly focusing on their insulation properties. A classification of bio-wastes is provided, namely of the lignocellulosic ones and their features and properties are described. Information about three main topics is collected: world production and consumption of some crops already used as building materials, their chemical composition and their most studied properties. Since the considered materials are lignocellulosic and they have many common features, a comparison is made. The aim is to have comparable information to support future research related to the production of eco-efficient indoor insulation boards. The result of this research is the choice of four different agro-industrial wastes produced in the Euro-Mediterranean Countries. This area was chosen as buildings typically have little or no insulation due to the regional mild climate; however, particularly with climate change, indoor hygrothermal comfort is poor. The collection of information allows some conclusions to be reached about the different bio-wastes already studied and identify gaps in the literature.
- Macrobiological Degradation of Esterified Wood with Sorbitol and Citric AcidPublication . Treu, Andreas; Nunes, Lina; Larnøy, ErikThere is a need for new solutions in wood protection against marine wood borers and termites in Europe. A new solution could be the esterification of wood with sorbitol and citric acid (SCA) since these are inexpensive and readily available feedstock chemicals and have shown protective properties against fungal wood degradation in earlier studies and prevented macrobiological degradation, as shown in this study. Protection of wood products in the marine environment lacks available wood preservatives that are approved for marine applications. Termite infestation is opposed mainly by biocide treatments of wood. Several wood modification systems show high resistance against both marine borers and subterranean termites. However, the existing commercialized wood modification products are costly. Both macrobiological forms of degradation represent a great threat for most European wood species, which are rapidly and severely degraded if not properly treated. This study investigated esterified wood in standard field trials against marine wood borers, and against subterranean termites in laboratory trials in a no-choice and choice test. The treatment showed good resistance against wood borers in the marine environment after one season and against subterranean termites in the laboratory after eight weeks. The low termite survival rate (SR) in the no-choice test during the first week of testing indicates a mode of action that is incomparable to other wood modification treatments.
- Impact of Water-Repellent Products on the Moisture Transport Properties and Mould Susceptibility of External Thermal Insulation Composite SystemsPublication . Roncon, Renata; Borsoi, Giovanni; Parracha, João Luís; Flores-Colen, Inês; Veiga, Rosário; Nunes, LinaExternal Thermal Insulation Composite Systems (ETICS) are constructive solutions widely used to increase the thermal insulation in new and retrofitted buildings. However, these systems can present several anomalies due to their constant exposure to weathering agents and anthropic factors. Water is generally the major cause of degradation. Thus, the application of water-repellent products can minimize the appearance of anomalies and increase the durability of the systems. In this paper, acrylic-based and siloxane-based hydrophobic products were applied to ETICS, with the aim of assessing the compatibility, effectiveness, and durability of these products. The moisture transport properties and mould susceptibility were assessed through laboratory tests on untreated and treated specimens. The durability of the hydrophobic treatments was also evaluated through artificial aging tests (heat-cold and freeze-thaw cycles). Results show that the protection products generally decreased water absorption, slightly decreased the drying rate, and presented adequate water vapor permeability. After aging, the products still had reasonable effectiveness and, with one exception, improved the water vapor diffusion of the systems. Additionally, ETICS underwent an alteration in the finishing coat (possible modification of the porosity) due to the aging cycles. No clear linear correlation was found between the contact angle values and water absorption results, evidencing the influence of other factors related to the composition of the water-repellent products.
- Characterization of the Mechanical Performance in Compression Perpendicular to the Grain of Insect-Deteriorated TimberPublication . Verbist, Maxime; Branco, Jorge M.; Nunes, LinaAmong biological agents, insect attacks may cause severe degradation of timber structures in the service life of buildings which leads to lower mechanical performance and, thus, maintenance problems over time. Additionally, compression perpendicular to the grain always features a weak spot with respect to the long-term mechanical performance of timber members and joints. In the present work, the respective strength and elastic modulus were thus investigated for insect deteriorated wood. Following a standardized geometry, small samples degraded by anobiids were extracted from beams made of sweet chestnut wood (Castanea sativa Mill.) that were removed from service. Visual assessment of the external wood surfaces was then performed to identify areas infested by insects. Afterwards, destructive monotonic compression tests were carried out perpendicularly to the grain on the damaged area to determine the loss of compressive strength and elastic modulus. The experimental results showed that the loss of compressive strength and elastic modulus might be linearly correlated to the wood density loss for small samples infested by insects. Nonetheless, future work should focus on determining accurately the density loss in the insect-deteriorated part through non- or semi-destructive tests, in order to establish stronger relationships with the mechanical properties loss investigated.
- Discussão de estratégias para a avaliação da biocolonização em ETICS : um caso de estudo em LisboaPublication . Borsoi, Giovanni; Parracha, João Luís; de Cooman, Quinten; Flores-Coles, Inês; Viegas, Cristina A.; Nunes, Lina; Moreira, Leonilde M.; Veiga, RosárioConservar e Reabilitar monumentos, edifícios e espaços são oportunidades únicas para fomentar a sustentabilidade dos territórios, constituindo-se o ENCORE 2020 - 4º Encontro de Conservação e Reabilitação de Edifícios numa ocasião ímpar para discutir os desafios da transformação no espaço construído: otimizar recursos, reutilizar materiais, melhorar a eficiência energética, repensar as centralidades urbanas, promover a resiliência. O presente documento junta os textos das comunicações apresentadas sobre a multiplicidade de aspetos que se entrecruzam no âmbito da intervenção no património construído, identificando, de forma multidisciplinar e sinergética, os desafios e os caminhos para melhor Conservar e Reabilitar.
- Performance parameters of ETICS : Correlating water resistance, bio-susceptibility and surface propertiesPublication . Parracha, João Luís; Borsoi, Giovanni; Flores-Colen, Inês; Veiga, Rosário; Nunes, Lina; Dionísio, Amélia; Gomes, M. Glória; Faria, PaulinaThe use of External Thermal Insulation Composite Systems (ETICS) significantly increased in the last decades due to their enhanced thermal properties, low installation cost and ease of application, not only in new constructions but also for thermal retrofitting of building facades. These multilayer rendering systems are constantly exposed to weathering agents and anthropic factors which can lead to physical-mechanical and aesthetical anomalies and thus affect their durability. However, possible synergetic effects among these agents are often neglected by international technical documents on the evaluation of the effectiveness and durability of ETICS. With the aim of filling this gap, moisture transport properties (capillary water absorption, water vapor permeability, water absorption under low pressure, and drying kinetics), thermal conductivity, mould susceptibility and surface properties (color, gloss, and roughness) of twelve commercially available ETICS were assessed and discussed. Possible links between these factors were analyzed and ETICS performance parameters were defined. Results demonstrate that a deeper knowledge of the correlation among ETICS properties can effectively contribute to the evaluation of the efficiency and long-term durability of these systems.
- Macro biological degradation of wood treated with sorbitol and citric acid : first results from marine environment and termite exposurePublication . Treu, Andreas; Nunes, Lina; Larnøy, ErikMost European wood species are rapidly and severely degraded in termite-infested areas and the marine environment. There is a need for new solutions, especially in the marine environment, since we lack wood preservatives approved for marine applications in Europe. Several wood modification systems show high resistance against both marine borers and subterranean termites. However, the existing commercialised methods of wood modification are costly. Therefore, a new, low cost and non-toxic wood modification system from inexpensive and readily-available feedstock chemicals have been used in this study. The treatment of wood with a combination of sorbitol and citric acid (PS-modification) showed good resistance against wood borers in the marine environment after one season and against subterranean termites in the laboratory after eight weeks. Future results from the ongoing field tests in the marine environment will reveal the long-term performance of PS-treated wood. The low termite survival rate in the non-choice test already in the first week of testing indicate a mode of action which is not comparable with other wood modification treatments.
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